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闭系震荡(盐)酸浸-煅烧(低温)纯化硅藻土研究
  • 分类:TQ424[化学工程]
  • 作者机构:[1]江西赣州技师学院,江西赣州341000, [2]江西理工大学材料科学与工程学院,江西赣州341000
  • 相关基金:国家自然基金项目(41062002):江西省科技厅资助项目(2008212);江西省教育厅资助项目(GJJ08287)
中文摘要:

采用闭系震荡酸浸和煅烧法对硅藻土进行提纯处理,通过X射线荧光光谱(XRF),扫描电镜(SEM)和Brunauer-Emmett-Teller(BET)法等手段对纯硅藻土进行表征。结果表明:提纯后,硅藻土SiO2含量提高至98%左右,Fe2O3等杂质含量显著减少,多孔构造高度发育,比表面有较大提高。

英文摘要:

Abstract: Diatomite was treated with hydrochloric acid by shaking technique at closed system and calcined to remove impurities. The chemical compositions of diatomite before and after purification were characterized using X-ray fluorescence spectrometry; the morphology and microstructure of purified diatomite investigated by scanning electron microscopy and N: adsorption-desorption isothemls; The investigations indicated that the content of SiO2 increases to 98 %, and oxide impurities were decreases after diatomite was purified; the integrity of the porous structure and specific surface area increases remarkably.

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