采用磷化处理后的还原铁粉,通过压制、热处理获得铁基软磁复合材料(ISMCs),探讨了成形压力和热处理工艺对材料磁导率、磁损耗和频率特性影响。研究结果显示,900MPa压力获得密度为7.2g/cm^3磁粉芯,振幅磁导率μa≥100(30~250kHz),且肛μa频率稳定性好(变化量≤0.02~0.03/kHz)。经400℃热处理后,肚。超过120(30~250kHz),提高了20%。热处理温度超过450℃,磁粉芯的磁损耗显著增加、肚。急剧下降。损耗分离研究显示,磁损耗增加主要体现在涡流损耗急剧上升。再经TG—DTA分析,磷化铁粉在462℃时出现一个明显的吸热峰,主要是磷酸氢盐发生分解反应,导致绝缘层破坏,进而影响材料的磁性能。
The iron-based soft magnetic composites(ISMCs) were prepared by pressing using phosphatizated reduced iron powder. Effects of the pressure and heat-treatment on the amplitude permeability, magnetic loss and frequency characteristics of ISMCs were discussed in this paper. Results shows that the density of ISMCs compressed under 900 MPa reaches 7.2 g/cm^3 ,and the amplitudeμa is higher than 100 (30-250 kHz) while frequency stability exhibits excellent (the p. change≤0.02-0.03/kHz). When ISMCs are heat-treated at 400℃ for 30 minutes,μa increases 20% and exceeds 120. But when the heat-treated temperature is above 450℃, the magnetic loss increases obviously andμa, decreases acutely. The separation of magnetic loss indicates that the increase of magnetic loss is attributed to the eddy current loss. The TG-DTA curves of the phosphatization powder shows an obvious endothermic peak at 462℃ ,and it means phosphates on the surface of powder decompose,which results the insulating film breakdown and magnetic properties deterioration.