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放电等离子制备Ti3AlC2/TiB2复合材料及性能
  • 期刊名称:硅酸盐学报35(5), 1-3,2007
  • 时间:0
  • 分类:TB333[一般工业技术—材料科学与工程]
  • 作者机构:[1]武汉理工大学,材料复合新技术国家重点实验室,武汉430070
  • 相关基金:国家自然科学基金(50572080);高等学校博士点基金(20050497002)资助项目.
  • 相关项目:Ti-Al-C系陶瓷/TiB2复合材料的制备与界面控制
中文摘要:

采用放电等离子烧结(spark plasma sintering,SPS)工艺制备了Ti3AlC2/TiB2复合材料,并研究了复合材料的性能。研究表明:在1250℃,30MPa烧结8min,可以获得相对密度达98%以上的致密Ti3AlC2/TiB2块体材料;在Ti3AlC2中添加TiB2能大幅度提高材料性能,当TiB2含量为30%(体积分数,下同)时,Ti3AlC2/30%TiB2复合材料的Vickers硬度达到10.39GPa,电导率为3.7×10^6v S/m;当TiB2含量为10%时,抗弯强度为696MPa,断裂韧性为6.6MPa.m^1/2。用电子显微镜对复合材料的显微结构分析表明:Ti3AlC2/TiB2复合材料的晶粒为层状结构。

英文摘要:

Ti3AlC2/TiB2 composites were prepared by the spark plasma sintering (SPS) process with different volume fractions of TiB2, and the properties of Ti3AlC2/TiB2 composites were investigated. The results indicated that the bulk Ti3AlC2/TiB2 with a relative density of 98% was fabricated by SPS under 30MPa and at 1 250℃ for 8min. The Vickers hardness, the flexural strength and fracture toughness and electric conductivity of Ti3AlC2/TiB2 composites are greatly enhanced with the addition of TiB2. The Vickers hardness and electric conductivity of Ti3AlC2/30%(in volume) TiB2 are 10.39 GPa and 3.7×10^6 S/m, respectively. When the volume fraction of TiB2 is 10%, the flexural strength and fracture toughness reach the maximum values, which are 696 MPa and 6.6 MPa·m^1/2, respectively. The microstructure characteristics of the Ti3AlC2/TiB2 composites were analyzed using an electron microscope. The results show that the grains of Ti3AlC2/TiB2 composites are structured in a layered form.

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