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高温固溶热处理对HIP态FGH96合金中碳化物影响规律的体视学研究
  • ISSN号:1001-4381
  • 期刊名称:《材料工程》
  • 时间:0
  • 分类:TG113.12[金属学及工艺—物理冶金;金属学及工艺—金属学]
  • 作者机构:[1]北京科技大学材料科学与工程学院,北京100083, [2]北京科技大学新金属材料国家重点实验室,北京100083, [3]钢铁研究总院高温材料研究所,北京100081
  • 相关基金:国家重点基础研究发展计划(973)资助项目(2010CB631204)
中文摘要:

利用金相显微镜,扫描电镜和透射电镜并结合体视学基本原理,对在不同固溶温度和冷却方式(空冷和炉冷)下热等静压(HIP)态FGH96合金中碳化物的数量、空间分布及尺寸分布等进行了定量表征和对比研究。结果表明:HIP态FGH96合金中碳化物主要为富Nb和Ti的MC,在原始颗粒边界(PPB)上分布的碳化物主要为块状,在PPB区域以外分布的碳化物主要由块状和花状MC组成。在1180℃以下进行固溶热处理时,碳化物含量增加并且加剧了合金中的PPB;当固溶温度达到1180℃以上时,随着固溶温度的升高,合金中碳化物数量减少,PPB逐渐消失。1200℃固溶后炉冷,固溶在基体中的碳主要以非PPB碳化物形式重新析出,会导致合金中PPB碳化物数量的降低,即使合金中的碳化物总量与固溶热处理前几乎相同。另外,空冷合金中PPB碳化物尺寸为单峰分布,而炉冷合金中则表现为双峰,后者与炉冷过程中碳化物能够重新析出密切相关。

英文摘要:

The OM, SEM, TEM and the stereology method were used to observe and quantitatively characterize the carbides in HIPed FGH96 alloys before and after high temperature solution treatment at different temperature. The results show that the carbides in HIPed FGH96 alloy are mainly MC type carbides which are rich in Ti and Nb. The shape of PPB carbides was block, while the non-PPB carbides were petal and block. Compared with the HIPed alloy, the amount of PPB carbides as well as the total carbides in FGH96 alloy increased when the heat treatment temperature was below 1180℃. But the amount of carbides decreased and the PPB gradually disappeared with the increasing tempera- ture when the heat treatment temperature was above 1180℃. The carbides precipitated mainly as non- PPB carbides if the HIPed alloy was furnace cooled. However, such re-precipitation was suppressed when the alloy was air cooled from the heat treatment temperature. Thus, when the alloy was either furnace or air cooled, the amount of PPB carbides was significantly reduced even the total amount of carbides retains almost the same as that in the HIPed alloy in case of furnace cooling. Moreover, the PPB carbide size distribution in the air cooling alloy appears a unimodal mode, while that in the fur-nace cooling alloy is a bimodal one, the latter of which was resulted from the re-precipitation of car- bides occurred in the furnace cooling process.

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期刊信息
  • 《材料工程》
  • 北大核心期刊(2011版)
  • 主管单位:中国航空工业集团公司
  • 主办单位:中国航空工业集团公司 北京航空材料研究院
  • 主编:曹春晓
  • 地址:北京市海淀区温泉镇环山村8号
  • 邮编:100095
  • 邮箱:matereng@biam.ac.cn
  • 电话:010-62496276
  • 国际标准刊号:ISSN:1001-4381
  • 国内统一刊号:ISSN:11-1800/TB
  • 邮发代号:
  • 获奖情况:
  • 国内外数据库收录:
  • 美国化学文摘(网络版),荷兰文摘与引文数据库,美国工程索引,美国剑桥科学文摘,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),中国北大核心期刊(2000版)
  • 被引量:16726