目的 研究露兜簕(Pandanus tectorius Soland.)茎皮的化学成分。方法 采用硅胶柱色谱、Sephadex LH-20柱色谱、高效液相色谱分离化合物,通过理化数据测定和波谱技术分析确定所得化合物的结构。结果 从露兜簕茎皮乙醇提取物中分离得到10个化合物,分别鉴定为:1'-O-benzyl-α-L-rhamnopyranosyl-(1″→6')-β-D-glucopyranoside(1),dihydrodehydrodiconiferyl alcohol(2),异牡荆素(3),牡荆素(4),3,5-二咖啡酰奎宁酸甲酯(5),3,5-二咖啡酰奎宁酸乙酯(6),3,4-二咖啡酰奎宁酸甲酯(7),(+)-lyoniresinol 3a-O-β-glucopyranoside(8),(-)-lyoniresinol 3a-O-β-glucopyranoside(9)和苄醇-β-D-吡喃葡萄糖苷(10)。结论 所有化合物均为首次从该植物中分离得到。
OBJECTIVE To study the chemical constituents in the stem barks of Pandanus tectorius Soland. METHODS The compounds were isolated by repeated chromatography. Their structures were elucidated by spectroscopic methods. RESULTS Ten compounds were isolated and identified as 1'-O-benzyl-α-L-rhamnopyranosyl-(1″→6')-β-D-glucopyranoside (1), dihydrodehydrodico- niferyl alcohol (2), isovitexin( 3 ), vitexin (4), 3,5-di-O-caffeoylquinic acid methyl ester( 5 ), 3,5-di-O-caffeoylquinic acid ethyl ester (6), 3,4-di-O-caffeoylquinic acid methyl ester(7), ( + )-lyoniresinol 3a-O-β-glucopyranoside(8), ( - )-lyoniresinol 3a-O-β-glucopy- ranoside (9) , and benzyl-β-D-glucopyranoside (10). CONCLUSION All compounds are isolated from this plant for the first time.