目的 建立一种简便、快速、可靠的检测生物检材中卡马西平的方法。方法 丙酮:水(v/v8:2)对生物检材进行浸泡,然后在p H=10~11的条件下,用乙酸乙酯进行提取分离,GC-MS对样品进行检测。结果 该方法简单易操作,背景干扰小,分离效果好,分析速度快。结论 该方法可用于法医毒物分析生物检材中卡马西平的检验,结果满意。
Objective To establish a simple, rapid and reliable method for the detection of C Masi Bing in biological samples. Methods Acetone:water (v/v 8:2) was soaked in biological samples, and then extracted and separated with ethyl acetate under the condition of pH=10 ~ 11, and the samples were detected by GC-MS. Results The method is simple and easy to operate, the background interference is small, the separation effect is good, and the analysis speed is fast. Conclusion This method can be applied to the analysis of C Masi Bing's test in the biological samples of forensic toxicological analysis, and the results are satisfactory.