采用湿法提纯工艺对广西田东膨润土进行提纯试验,研究了分散剂的类型及用量、液固质量比及分散条件对提纯效果的影响。结果表明田东膨润土最佳提纯工艺参数为:分散剂为六偏磷酸钠、分散剂用量为1%、最佳液固质量比为10∶1、料浆温度为60℃、搅拌转速为500r/min、搅拌时间为60min。提纯产物的胶质价为88.6mL/15g,膨胀容为90.5mL/g,阳离子交换量为95.8mmol/100g,蒙脱石质量分数由70%提高到97%。
Tests on bentonite from Tiandong, Guangxi were conducted by the wet purification process and influence factors such as type and dosage of dispersants, liquid-solid ratio, dis- persion conditions on the purification effect was investigated. The results indicate that the optimum conditions for purification are the dosage of dispersant of sodium hexametaphosphate being 10%, the liquid-solid ratio 10 : 1, the temperature of slurry 60 ℃,the speed of stirring 500 r/min and the time of stirring 60 minutes, the colloid index of purified product 88.6 mL/15 g, the expansion capacity 90. 5 mL/g, the cation exchange capacity (CEC) 95.8 retool/100 g and the increase of content of montmorillonite to 97% from 70%.