中文摘要：

目的：建立快速测定香精香料复杂基体中甜蜜素添加量的方泫。方法：对样品进行柱前衍生化处理，选择C18柱和70：30（V／V）的乙腈一水为流动相，利用二极管阵列检测器（DAD）在314nm波长处进行检测。结果：本法可有效消除香精香料中甜蜜素检测的假阳性问题，测得的峰面积与甜蜜素质量浓度（在2．5-250mg／L范围内）呈线性关系，相关系数为0．9992，甲均回收率为94．22％497．19％。结论：本方法简便、快速、准确且重现性好，能准确地对香精香料复杂基体中的甜蜜素进行定性和定量分析。

英文摘要：

Objective： To establish a method for rapid determination of sodium cyclamate in food flavors and fragrances that are very complex substances. Methods： Samples were subjected to precolumn derivatization. The chromatographic separation was achieved on a C18 column with a mobile phase consisting of a mixture of acetonitrile and water （70：30, V/V） and the analyte was detected with a DAD detector set at 314 nm. Results： The analytical method developed was shown to result in an effective elimination of false positive detection for sodium cyclamate in food flavors and fragrances. A good linear relationship was observed between HPLC peak area and sodium cyclamate concentration in the range of 2.5 - 250 mg/L with the correlative coefficient of 0.9992, and the average recoveries were in the range of 94.22%-97.19%. Conclusion： This method is simple, rapid, accurate and repeatable, and applicable for qualification and quantification of sodium cyclamate in food flavors and fragrances.