目的:测定峨眉产黄连药材的水分、灰分和浸出物,为建立峨眉产黄连药材质量标准提供依据。方法:按《中国药典》(2010版一部)对黄连中的水分、灰分及浸出物进行测定,并对浸出物的提取条件进行优化。结果:测得黄连药材水分11.68%-19.04%,总灰分2.51%-3.79%,酸不溶性灰分0.34%-1.48%,醇溶性浸出物量24.82%-36.14%。结论:峨眉产黄连药材水分不超过14%,总灰分不高于5%,酸不溶性灰分不高于1%,醇溶性浸出物量不低于15%。
Obj ective:To determine the moisture,ashes,and extracts from the Coptidis Rhizoma for establishing of quality standards.Methods:According to the procedures recorded in Chinese Pharmacopoeia,published in 2010,moisture, ashes and extracts of samples were measured respectively.And the extraction conditions of extract was optimized.Results:The moisture in E’mei Coptidis Rhizoma was 11.68%-19.04%,the total ashes content was 2.51%-3.79%,the acid insoluble ash content was 0.34%-1.48%,and the content of ethanol extract was 24.82%-36.14%.Conclusion:The moisture in E’mei Coptidis Rhizoma was less than 14%,the total ashes content was less than 5%,with the acid insoluble ash content was less than 1%,the content of ethanol extract was not less than 1 5%.