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Sc微合金化纯铝大变形组织与强化机制
  • ISSN号:0258-7076
  • 期刊名称:《稀有金属》
  • 时间:0
  • 分类:TG146.2[金属学及工艺—金属材料;一般工业技术—材料科学与工程;金属学及工艺—金属学]
  • 作者机构:江苏大学先进制造与现代装备技术工程研究院,江苏镇江212013
  • 相关基金:国家自然科学资金项目(51074079); 江苏省高校科研成果产业化推进项目(JH10-37); 江苏大学“拔尖人才培养工程”基金项目(1211110001)资助
中文摘要:

以工业纯铝和Al^-1%Sc合金为原料,通过熔炼得到Sc微合金化纯铝(Al-0.1%Sc)。采用X射线衍射(XRD)分析、电子背散射衍射(EBSD)分析技术以及拉伸实验,研究了Al-0.1%Sc合金在等通道转角挤压(ECAP)和压缩大应变加工过程中的组织演变和强化机制。ECAP试验采用工艺路线Bc进行3道次挤压加工,即每次挤压后将工件沿轴线方向旋转90°,旋转方向不变,挤压速度为5 mm·s^^-1。结果表明:ECAP加工使得合金平均晶粒尺寸减小,晶粒尺寸基本被细化到4 mm以下;显著提高了合金强度,抗拉强度由105 MPa提高到162 MPa;降低了合金中低角度晶界比例,从0.889减小到0.652;使得合金内部积累了一定量的位错,位错密度为0.5321014 m^-2。而后续的压缩大应变加工对合金的平均晶粒尺寸几乎没有影响,使得合金的抗拉强度提高到176 MPa,使得合金的低角度晶界比例提高到0.765,使得合金的位错密度提高到1.7151014 m^-2。大应变Al-0.1%Sc合金的强化主要由晶格摩擦应力、位错强化、低角度晶界强化和高角度晶界强化组成,其中低角度晶界和位错的强化贡献占绝大部分。

英文摘要:

The Sc-microalloyed pure aluminum(Al^-1% Sc) was made from industry pure aluminum and Al^-1% Sc alloy by melting.Microstructure evolution and strengthening mechanisms of Al-0. 1% Sc alloy during equal-channel angular pressing(ECAP) and compressing were researched by X-ray diffraction(XRD),electron backscattered diffraction(EBSD) analysis and tensile test. In the ECAP test,the process Route Bc was used to carry out the 3 passes extrusion process,and the extrusion speed was 5 mm·s^^-1. In the process Route Bc,the workpiece would be rotated 90° along the axis after each extrusion and the direction of the rotation was constant.The results indicated that the Al-0. 1% Sc alloys processed by ECAP had a reduction on grain size and most grains were refined to4 mm or less,and the tensile strength was improved from 105 to 162 MPa. The proportion of low angle grain boundary of the Al-0. 1%Sc alloys processed by ECAP was lower and it was reduced from 0. 889 to 0. 652. There was a certain amount of dislocation in the Al-0. 1% Sc alloys processed by ECAP and the dislocation density was 0. 5321014 m^-2. The subsequent compressing large strain processing almost had no effect on the average grain size of the alloy. The tensile strength and the proportion of low angle grain boundary after the compressing large strain processing were respectively increased to 176 MPa and 0. 765. And the subsequent compressing large strain processing increased the dislocation density to 1. 7151014 m^-2. Strengthening contributions of large strain Al-0. 1% Sc alloy were mainly from lattice friction stress,dislocation strengthening,low angle grain boundary and high angle grain boundary strengthening.And low angle grain boundary and dislocation strengthening were dominant.

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期刊信息
  • 《稀有金属》
  • 中国科技核心期刊
  • 主管单位:中国科学技术协会
  • 主办单位:北京有色金属研究总院
  • 主编:屠海令
  • 地址:北京新街口外大街2号
  • 邮编:100088
  • 邮箱:xxsf@grinm.com
  • 电话:010-82241917 62014832
  • 国际标准刊号:ISSN:0258-7076
  • 国内统一刊号:ISSN:11-2111/TF
  • 邮发代号:82-167
  • 获奖情况:
  • 中文核心期刊,冶金工业类核心期刊,中国科技论文统计源期刊
  • 国内外数据库收录:
  • 俄罗斯文摘杂志,美国化学文摘(网络版),荷兰文摘与引文数据库,美国工程索引,美国剑桥科学文摘,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),中国北大核心期刊(2000版)
  • 被引量:13688