渗入散开的一个新方法被用来综合 macroscopicalpha-Zr (C6H5PO3 ) 2 (alpha-ZrBP ) 试管。比作平淡的方法,没有 HF 被使用,有在长度的几毫米的 fiberlikeproduct 是结果显示的 obtained.SEM (扫描电子显微镜学) 这些纤维是试管。试管的墙与对方一起由 alpha-ZrBPoverlapped 的薄片组成。当我们知道,它是 alpha-ZrBP 的 millimeter-scalesupramolecular 汇编的合成上的第一份报告。
A new method of infiltration-diffusion is used to synthesize macroscopic α-Zr(C6H5PO3)2 (α-ZrBP) tube. Compared to the routine method, no HF was used and a fiberlike product with several millimeters in length was obtained. SEM (scanning electronic microscopy) result indicates that these fibers are tubes. The wall of the tubes is composed of the flake of α-ZrBP overlapped with each other. As we know, it is the first report on the synthesis of millimeter-scale supramolecular assembly of α-ZrBP.