中文摘要：

系统地建立了一套简单、快速、能同时定量分析甲苯液相催化氧化主要产物苯甲醛、苯甲醇及苯甲酸的气相色谱分析方法。采用FFAP毛细管柱和氢火焰离子化检测器（FID），以邻硝基甲苯为内标标定苯甲醛、苯甲醇，以邻苯二甲酸二甲脂为内标标定苯甲酸。结果表明，苯甲醛、苯甲醇、苯甲酸样品的平均回收率和标准偏差（RSD）分别为105．39％，101．94％，97．18％和3．19％，3．71％，1．66％。该分析方法简单、快速、精度高。

英文摘要：

A specific GC analysis method was established for the rapid quantification of the main products of liquid-phase oxidation of toluene, namely, benzaldehyde, benzyl alcohol and benzoic acid. A GC equipped with a FFAP capillary and a FID detector was adopted. O-nitrotoluene and dimethylphthalate were used as internal standards of benzaldehyde, benzyl alcohol and benzoic acid respectively. The results indicated that the mean recovery rate for spiked samples are 105.39%, 101.94%, 97. 18%, respectively, and the standard deviations are 3. 19%, 3.71%, 1.66%, respectively.