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中文摘要：
应用电化学方法制备Zn-Ni合金晶须.样品的成分、形貌用XRD、SEM、EDS等方法表征,结果表明,晶须的物相是Ni5Zn21和Ni3Zn22,直径250 nm,长度2-4μm,长径比8-16.同时用循环伏安法探讨了该过程的电化学行为.为晶须的制备提供了一种新的方法.
英文摘要：
The Zn-Ni alloy whiskers were prepared by electrochemical method and were characterized by XRD. SEM and EDS methods. The results showed that Ni5Zn21 and Ni3Zn22 whiskers were obtained with the length of 2 -4 um and the diameter of 250 nm,thereby the rations of length/diameter fell between 8 and 16. The electrochemical behavior was investigated by cyclic voltammetry method simultaneously. A new method was provided on whisker preparation based on this work.
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