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一步法合成双亲的Ag，Cu，Cd和Ni纳米金属单质
  • ISSN号：1001-4861
  • 期刊名称：《无机化学学报》
  • 时间：0
  • 分类：O614.123[理学—无机化学;理学—化学] O614.121[理学—无机化学;理学—化学]
  • 作者机构：[1]吉林大学化学学院、无机合成与制备化学国家重点实验室,长春130012
  • 相关基金：国家自然科学基金资助项目（No.20331010）.
作者： 李新昊[1], 曹学静[1], 张东慧[1], 陈接胜[1]
关键词： 溶剂热法, 过渡金属, 纳米结构, 双亲, solvothermal, transition metal, nano-structure, amphiphilic
中文摘要：

本文报道利用简单的溶剂热方法，以相应的金属盐作为唯一的反应物来制备Ag，Cu，Cd，Ni等纳米结构金属。采用XRD，SEM．TEM等测试手段对产物进行了表征。实验结果表明，反应条件特别是反应时间对产物最后的化学组成起重要作用。该制备方法具有一定的普适性，而且简单实用；涉及的反应条件相对温和，获得的产物具有双亲性质，能均匀分散于大部分极性和非极性溶剂中。

英文摘要：

Nanostructured Ag, Cu, Cd, Ni were synthesized using the corresponding metal salts as mono-precursors via a facile solvothermal method, and the products were characterized by XRD ,SEM and TEM. It is proved that the reaction time plays a key role in determining the composition of the products. This simple and general process is environment-friendly, and the products obtained are amphiphilic and dispersible well in most of the polar and nonpolar solvents.

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期刊信息
  • 《无机化学学报》
  • 中国科技核心期刊
  • 主管单位:中国科学技术协会
  • 主办单位:中国化学会
  • 主编：游效曾
  • 地址：南京市南京大学仙林区化学楼
  • 邮编：210023
  • 邮箱：wjhx@nju.edu.cn
  • 电话：025-89682307
  • 国际标准刊号：ISSN：1001-4861
  • 国内统一刊号：ISSN：32-1185/O6
  • 邮发代号:28-133
  • 获奖情况:
  • 2007年获江苏省优秀期刊奖,2009年获华东地区优秀期刊奖
  • 国内外数据库收录:
  • 美国化学文摘（网络版）,荷兰文摘与引文数据库,美国科学引文索引（扩展库）,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊（2004版）,中国北大核心期刊（2008版）,中国北大核心期刊（2011版）,中国北大核心期刊（2014版）,英国英国皇家化学学会文摘,中国北大核心期刊（2000版）
  • 被引量:19587