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中文摘要：
通过二碘化钐催化的Biginelli反应合成了5-乙酰基-6-甲基-4-（2-呋喃基）-3，4-二氢嘧啶-2-酮，并采用单晶X-射线衍射法测定了其晶体结构．晶体属单斜晶系，P21／n空间群，a=0．8837（2）nm，b=0．8186（2）nm，c=1．4831（3）nm，β=103．73（5）°，V=1．0422（4）nm^3，Mr=220．23，Z=4，Dc=1．404g／cm^2，μ（MoKα）=0．104mm^-1，F（000）=464．最终偏离因子为R=0．0623、wR=0．1384．
英文摘要：
The title compound 5-acetyl-6-methyl-4- （2-furyl） -3,4-dihydropyrimidine-2 （H） -one was synthesized by samarium diiodide catalyzed Biginelli reaction, a one-pot condensation of 2-furaldehyde, urea and 2,4-pentanedione. The crystal structure was determined by X-ray single-crystal diffraction analysis. The crystal belongs to monoclinic, space group P21/n with unit cell dimensions a = 0. 883 7（2） nm, b = 0. 818 6（2） nm, c = 1.483 1（3） nm,/3 = 103.73（5）°, V = 1.042 2（4） nm^3, Mr= 220.23, Z = 4, Dc= 1.404g/cm^3,μ（MoKα） = 0.104mm^-1, F（000） = 464. The final R = 0. 062 3 and wR = 0. 138 4 for 1 820 observed reflections with I 〉 2σ（1）.
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