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Cu/Ni和Cu/Nb纳米多层膜的应变率敏感性
  • ISSN号:0412-1961
  • 期刊名称:《金属学报》
  • 时间:0
  • 分类:TB383[一般工业技术—材料科学与工程]
  • 作者机构:装甲兵工程学院装备维修与再制造工程系,北京100072
  • 相关基金:国家自然科学基金项目Nos.51401238和51102283
中文摘要:

为研究调制周期和界面结构对纳米多层膜应变率敏感性的影响,采用电子束蒸发镀膜技术在Si基片上制备了不同周期(Λ=4 nm,12 nm,20 nm)的Cu/Ni纳米多层膜,采用磁控溅射技术在Si基片上制备了不同周期(Λ=5 nm,10 nm,20 nm)的Cu/Nb纳米多层膜。在真空条件下,对Cu/Ni纳米多层膜进行了温度分别为200和400℃、时间4 h的退火处理,对Cu/Nb纳米多层膜进行了温度分别为200、400和600℃,时间为4 h的退火处理。采用XRD和TEM表征了Cu/Ni和Cu/Nb纳米多层膜的结构,采用纳米压痕仪获取了不同加载应变率(0.005、0.01、0.05和0.2 s^-1)下纳米多层膜的硬度。结果表明,应变率敏感性受到界面结构和晶粒尺寸的影响,非共格界面密度提高以及晶粒尺寸变大均可导致应变率敏感性下降。当周期变大时,Cu/Ni纳米多层膜的非共格界面密度提高,晶粒尺寸变大,应变率敏感性指数m减小;当周期变大时,Cu/Nb纳米多层膜的非共格界面密度下降,晶粒尺寸变大,m基本不变。随退火温度上升,Cu/Ni和Cu/Nb纳米多层膜应变率敏感性大体上呈现下降趋势,这是由退火过程中非共格界面密度上升和晶粒长大共同引起的。

英文摘要:

Different from monolayers of same components, nanoscale multilayers have different mechanical properties owing to their relatively high interfacial density, such as extremely high yield strength,high ductility and outstanding wear resistance. Furthermore, their precise modulation period and unique interfacial structures contribute to investigate the plastic deformation mechanism of metal materials. As the plastic deformation behaviors of nanoscale multilayers were reflected in a thermal activation process,strain rate sensitivity index m can be used to characterize the tendency of material strengthening as the strain rate increases. To investigate the impacts of modulation period and interfacial structures upon strain rate sensitivity of nanoscale multilayers, Cu/Ni nanoscale multilayers with different periods(L=4 nm,12 nm, 20 nm) were prepared on Si substrate with e-beam evaporation technologies, while Cu/Nb nanoscale multilayers with different periods(L=5 nm, 10 nm, 20 nm) were prepared on Si substrate with magnetron sputtering technologies. Under vacuum conditions, the Cu/Ni nanoscale multilayers of different periods were annealed at 200 and 400 ℃ for 4 h respectively, and the Cu/Nb nanoscale multilayersof different periods were annealed at 200, 400 ℃ and 600 ℃ for 4 h respectively. Microstructures of Cu/Ni and Cu/Nb nanoscale multilayers were characterized with XRD and TEM. Besides, the hardness of nanoscale multilayers was measured by nano-indentation techniques under different loading strain rates(including 0.005, 0.01, 0.05 and 0.2 s^-1). The results suggested that strain rate sensitivity was impacted by interfacial structures and grain size. Both increased density of incoherent interfaces and grain size could result in weaker strain rate sensitivity. As the period increases, the density of incoherent interfaces and the grain size of Cu/Ni nanoscale multilayers increased, leading to a decline in the strain rate sensitivity.While for Cu/Nb nano scale multilayers, the density of incoherent i

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期刊信息
  • 《金属学报》
  • 中国科技核心期刊
  • 主管单位:中国科学协术协会
  • 主办单位:中国金属学会
  • 主编:柯俊
  • 地址:沈阳文化路72号
  • 邮编:110016
  • 邮箱:shxiao@imr.ac.cn
  • 电话:024-23971286
  • 国际标准刊号:ISSN:0412-1961
  • 国内统一刊号:ISSN:21-1139/TG
  • 邮发代号:2-361
  • 获奖情况:
  • 第一、二届全国优秀科技期刊评比一等奖,第一、二、三届国家期刊奖,国家期刊方阵"双高"期刊,第一、二、三届中国科学院科技期刊评比一等奖,中国科学院优秀期刊特别奖,第一、二、三、五届中国科协优秀科技期刊评比一等奖,中国科协精品期刊工程A类、B类,第一、二、三、四、五届中国百种杰出学术期刊,首届出版政府奖
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  • 被引量:26785