中文摘要：

以CuCl2·2H2O为铜源，InCl3·4H2O为铟源，L-半胱氨酸为硫源，N，N二甲基甲酰胺（N，N—dimethylformamide，DMF）为溶剂，在180℃下反应16h合成了CulnS2微晶。用X射线粉末衍射仪、X射线光电子能谱、场发射扫描电子显微镜对产物的结构、形貌、相组分进行表征。结果表明产物是由厚度为10～50nm纳米片组成的球状CulnS2微晶。并对由纳米片组成的球状CulnS2微晶的形成机理进行了简单探讨。

英文摘要：

Copper indium sulfide product was synthesized via a mild solvothermal approach （at 200 ℃for 25 h ） with CuCl2·2H2O as the copper source, InCl3·4H2O as the indium source, L-cysteine as the sulfur source, and N, N-dimethylformamide as the reaction medium Morphology, structure, and phase constituents of the as-prepared CuInS2 product was characterized by X-ray diffraction （XRD）, X-ray photo-electron spectroscopy （XPS） and field-emission scanning electron microscopy （FESEM）. Results show that the CuInS2 product had ball-like morphology composed of large numbers of nanoplates and the thickness of CuInS2 nanoplates was found to vary from 10 nm to 50 nm. A possible formation mechanism of the CulnS2 product with ball-like morphology was put forward and briefly discussed based on the experimental results.