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中文摘要：
以胶原纤维为模板，首先将Zr（Ⅳ）负载在胶原纤维上，然后吸附磷，最后经高温煅烧除去胶原纤维模板制备了介孔磷酸锆钠（NaZr2（PO4）3，NZP）。利用电感耦合等离子发散光谱仪（ICP）、X射线衍射仪（XRD）、场发射透射电镜（FETEM）、X射线光电子能谱（XPS）、傅立叶变换红外光谱（FT-IR）、N2吸附／脱附分析等对NZP进行了表征。结果表明，胶原纤维模板在800℃时即可完全去除，并形成介孔结构；当以磷酸二氢纳（NaH2PO4）为磷源、n（Zr）／n（P）=0．62时，经800℃煅烧得到了介孔率为97％的NZP。
英文摘要：
The mesoporous NaZr2 （PO4）3 （NZP） is prepared using collagen fiber as template. The Zr（ Ⅳ ） is first loaded on collagen fiber and then the phosphate is adsorbed. This precursor is heat treated and the mesoporous NZP is obtained. Inductive coupled plasma emission spectrometer （ICP）, X-ray diffraction（XRD）, field emission transmission electron microscope（FETEM）, X-ray photoelectron spectroscopy（XPS）, fourier transform infrared spectrometer（FT-R） and N2 adsorption/desorption techniques are used to characterize synthesized mesoporous NZP. The experimental results indicate that the collagen fiber template can be completely removed at 800℃, as a consequence the NZP with mesoporous structure is obtained. It is found that the mesopore extent of NZP is 97% using Nail2 PO4 as phosphate source and n（Zr）/n（P）=0. 62.
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