采用水热合成方法在透明导电玻璃上制备了TiO2纳米棒阵列,利用扫描电子显微镜(SEM)和X射线衍射仪(XRD)等手段对样品进行分析和表征。研究了盐酸浓度对阵列形貌和结构的影响,并针对其影响机理做了进一步的探讨。结果表明,TiO2纳米棒为金红石相,在盐酸与去离子水的比例为1.0时,TiO2纳米棒阵列生长方向垂直于衬底,排列整齐,组织均匀致密。
Highly ordered TiO2 nanorod arrays were prepared on glass substrate by using hydrothermal method.The characterization of TiO2 nanorod arrays was studied by using scanning electron microscope(SEM) and X-ray diffraction(XRD) analysis.Results showed that TiO2 nanorod arrays had highly crystallized rutile phase,better verticality on the substrate and density arrays when ratio of acid to deionized water was 1.0.