研究了取向硅钢制备过程中常见的两种冷轧工艺,主要研究了一阶段冷轧与两阶段冷轧+中间退火工艺对初次再结晶组织及织构的影响.结果表明:采用两阶段冷轧+中间退火工艺制备以Cu2S为主抑制剂的取向硅钢,其初次再结晶平均晶粒尺寸为18.1μm,高斯晶粒的体积分数为0.6%,迁移性强的重位点阵晶界(∑5+∑9)和高能晶界(20°-45°取向偏差角)所占比例分别为1.8%和50.4%.与一阶段冷轧工艺相比,其初次再结晶晶粒较细,且高斯晶核与特征晶界所占的比例较高,有利于高斯晶粒发生二次再结晶.
Two common cold-rolling processes of grain oriented silicon steel and the effects of the single stage cold rolling and two-stage cold rolling with intermediate annealing processes on the primary recrystallization microstructure and texture were investigated. The results revealed that for the grain oriented silicon steel prepared under the two-stage cold rolling process with intermediate annealing with CuE S as the main inhibitor, the average grain size of the primary recrystallization microstructure was 18.1 μm, the volume fraction of Goss grain was 0. 6% , the ratio of coincidence site lattice (CSL, ∑ 5 + ∑9 )and high energy grain boundaries (20 ~ 45° misorientation angles )which have the higher migration than the conventional boundaries were 1.8% and 50.4% , respectively. Compared with the single stage cold rolling process, the primary recrystallization grains of the two-stage cold rolling with intermediate annealing were finer; moreover, the proportion of Goss grain and high migration boundaries were larger, which were favorable to the secondary recrystallization occurrence of the Goss grain.