中文摘要：

采用抑制型电导离子色谱法检测电镀液中的常见阴离子．色谱条件是：IonPacAS11-HC阴离子交换色谱柱，淋洗液自动发生装置在线产生KOH梯度淋洗，抑制型电导检测．检测限（S／N=3）在0．29-15．3μg·l^-1，阴离子F^-，Cl^-，MSA^-，NO3^-，SO4^2-，PO4^3-和CrO4^2-的线性范围均在两个数量级以上，RSD在5％以下，回收率为92％-110％，具有灵敏度高，选择性好，重现性佳等特点，用于实际样品的检测，结果令人满意．

英文摘要：

Anions in plating relative solutions were separated by ion chromatography and detecting anions by suppressed conductivity detector simultaneously. The separations of common anions were obtained by IonPac AS11-HC column which is a high capacity anion-exchange column and KOH gradient which was generated by EG50 Eluent Generator was selected. The method detection limit（ S/N =3 ）for all seven anions are from 0. 29μg·l^-1 to 15.3μg·l^-1 ; all seven calibration curvesare linear over two orders of magnitude; RSDs are lower than 5 % while the recoveries are between 92 % and 110 %. This method possesses of the advantages of high sensitivity, distinguished selectivity, good reproductivity and being friendly to the environment.