利用X射线衍射技术(XRD)测试了涂层及其基体材料的应力及其变化规律,建立了一种涂层结合界面应力检测系统,进行界面结合状态的检测研究.利用涂层从基体脱粘前后的界面应力变化量,结合涂层材料的物性参数和涂层-基体系统温度场参数,用涂层残余应力衍射峰来表征涂层与基体的结合强度,创立一种研究检测涂层结合强度理论的实验新方法,适用于各种热障涂层的界面结合强度测量.
Stresses and its variation of coating and matrix are measured by XRD (X-ray diffraction). A test system that measures coating stress on the bonding interface is established, and the measurement of interface bonding status is researched. By using interfacial stress variation before and after coating debonding from matrix, combined with the physical parameters of coating material and temperatures field parameter of coating-matrix system, the bonding strength of coating-matrix is represented by the diffraction peak of coating residual stress. A new experiment method to measure bonding strength of coating and matrix is introduced which is applicable to measuring interfacial bonding strength of all kinds of polycrystalline thermal barrier coatings.