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多孔氧化铝模板结合sol-gel旋转涂敷法制备PZT纳米管
  • ISSN号：1001-9731
  • 期刊名称：功能材料
  • 时间：2012.6.6
  • 页码：1605-1609
  • 分类：TB383.1[一般工业技术—材料科学与工程]
  • 作者机构：[1]南京理工大学软化学与功能材料教育部重点实验室 南京大学物理学院固体微结构物理国家重点实验室
  • 相关基金：国家自然科学基金资助项目(51077072,10874065,61171043)
  • 相关项目：电解-电化学混合电容器纳米电极的制备及电性能研究
作者： 宋晔|蒋龙飞|戚卫星|路超|朱绪飞|杭启明|朱信华|SONG Ye1,JIANG Long-fei1,QI Wei-xing1,LU Chao1,ZHU|2.National Laboratory of Solid State Microstructur|
关键词： 氧化铝模板, Sol-gel法, PZT, 纳米管, 制备
中文摘要：

利用溶胶-凝胶旋转涂敷法在通孔的多孔阳极氧化铝(PAA)模板中制备了锆钛酸铅(PZT)纳米管,研究了溶胶浓度对样品形貌的影响。利用SEM和TEM观察了纳米管阵列和单根纳米管的形貌,采用XRD和EDS图谱分析了纳米管的相结构和化学元素组成。结果表明合成的PZT纳米管结晶良好,具有钙钛矿结构(属于四方晶系);纳米管具有较高的韧性但表面较粗糙,直径和管壁厚度分别约为75和7nm,直径与原始PAA模板的孔径相吻合。在一定范围内调节PZT溶胶的浓度(0.1～0.4mol/L),均能在PAA模板的孔洞中形成PZT多晶纳米管,且组成PZT纳米管的晶粒随着溶胶浓度的增加而变大。

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期刊信息
  • 《功能材料》
  • 北大核心期刊（2011版）
  • 主管单位:重庆材料研究院
  • 主办单位:重庆材料研究院
  • 主编：黄伯云
  • 地址：重庆北碚区蔡家工业园嘉德大道8号
  • 邮编：400707
  • 邮箱：gnclwb@126.com
  • 电话：023-68264739
  • 国际标准刊号：ISSN：1001-9731
  • 国内统一刊号：ISSN：50-1099/TH
  • 邮发代号:78-6
  • 获奖情况:
  • 2008、2011年连续获中国精品科技期刊,2010获重庆市双十佳期刊
  • 国内外数据库收录:
  • 美国化学文摘（网络版）,荷兰文摘与引文数据库,美国工程索引,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊（2004版）,中国北大核心期刊（2008版）,中国北大核心期刊（2011版）,中国北大核心期刊（2014版）,英国英国皇家化学学会文摘,中国北大核心期刊（2000版）
  • 被引量:30166