应用一维1HNMR、13CNMR、DEPT、二维HMBC、HSQC、1H—HCOSY、ROESY对1,3,6-三羟基-7-甲氧基-2,8双(3-甲基-2-丁烯)-9劬酮(amangostin、α-MAG)的1H、13C原子进行了指认归属.
The fruit hull of mangosteen, Garcinia mangostana, has been used for many years as a medicine for treatment of skin infection, wounds and diarrhea. In the present study, 1D 1H NMR, 13C NMR, DEPT and 2D HMBC, HSQC, 1H-1H COSY, ROESY methods were used to identify the structure of 1,3,6-trihydroxy-7-methoxy-2,8-bis-(3- methyl-2-butenyl)-9-xanthenone α-mangostin extracted from the fruit hull of mangosteen. The 1H and 13C chemical shifts of α-mangostin were assigned.