试图从野 Sargentodoxa cuneata 的水溶性的部分学习化学成分。混合物被硅石胶化和 HW-40C 列层析孤立的方法。他们的结构被阐明根据光谱 ESIMS 和 NMR 的分析。结果八已知的 glycosides 是被孤立并且识别()-lyoniresinol-9-O--D-glucoside (1 ) ,(+)-lyoniresinol-9-O--D-glucoside (2 ) ,()-lyoniresinol-9-O--D-glucoside (3 ) ,(+)-syringaresinol-4-O--D-glucoside (4 ) , androsin (5 ) ,(+)-syringin (6 ) , sargentol (7 ) 和 daucosterol (8 ) 。结论混合物 1, 3 和 6 第一次从这植物被孤立,并且野 S 的水溶性的部分的成分。cuneata 第一次系统地被学习。
AIM: To study the chemical constituents from the water-soluble fraction of wild Sargentodoxa cuneata. METHODS: The compounds were isolated by silica gel and HW-40C column chromatography. Their structures were elucidated on the basis of spectral analysis of ESI-MS and NMR. RESULTS: Eight known glycosides were isolated and identified as (-)-lyoniresinol-9-O-β-D-glucoside (1),(+)-lyoniresinol-9-O-β-D-glucoside (2),(-)-lyoniresinol-9′-O-β-D-glucoside (3), (+)-syringaresinol-4-O-β-D-glucoside (4), androsin (5), (+)-syringin (6), sargentol (7) and daucosterol (8). CONCLUSION: Compounds 1, 3 and 6 were isolated from this plant for the first time, and constituents of the water-soluble parts of wild S. cuneata were studied systematically for the first time.