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由伴生明矾石尾矿制备铝钾产品
  • ISSN号：1009-606X
  • 期刊名称：过程工程学报
  • 时间：2013.4.15
  • 页码：224-229
  • 分类：TF111[冶金工程—冶金物理化学]
  • 作者机构：[1]低品位难处理黄金资源综合利用国家重点实验室,紫金矿业集团股份有限公司,福建上杭364200, [2]湿法冶金清洁生产技术国家工程实验室,中国科学院过程工程研究所,北京100190
  • 相关基金：低品位难处理黄金资源综合利用重点实验室开放基金资助项目（编号：ZJKY2011（B）KFJJ002）; 国家杰出青年科学基金资助项目（编号：51125018）; 国家自然科学基金重大项目资助（编号：51090380）
  • 相关项目：碱熔盐活化分解红土镍矿及硫酸低压浸出镍、钴的基础研究
作者： 宋静|郭强|阮仁满|齐涛|
关键词： 明矾矿, 焙烧, 酸浸, 结晶, AL, K, alunite, calcination, acid leaching, crystallization, Al, K
中文摘要：

提出了伴生明矾石矿尾矿中温焙烧低浓度酸浸处理工艺,尾矿经700℃焙烧3h后,在液固比为6mL/g,10%硫酸中90℃水溶搅拌3h,Al和K浸取率分别达83%和93%.通过自然结晶和蒸发结晶分别得到了明矾和水合硫酸铝晶体,出钒率超过20%,以氧化物记的明矾及水合硫酸铝的回收率均达到65%左右,初步实现了铝、钾产品的分离,在保持较高Al,K浸取率的前提下降低了能耗、酸耗.

英文摘要：

A medium temperature calcination-low concentration acid leaching process was introduced to treat the associated alunite ore tailings. After calcination of the tailings at 700℃ for 3 h, and following leaching at 90℃ for 3 h in 10% sulfuric acid system with the acid/ore ratio of 6 mL/g, the leaching rates of Al and K reached 83% and 93%, respectively. Alum and aluminum sulfate hydrate crystals were obtained through natural and evaporation crystallization. The recovery rate of alum and aluminum sulfate hydrate crystals was up to 65%. This work provides a method to separate aluminum and potassium products preliminarily under the premise of reduction of energy and acid consumption.

同期刊论文项目
碱熔盐活化分解红土镍矿及硫酸低压浸出镍、钴的基础研究
期刊论文 27 会议论文 3
湿法冶金
期刊论文 108 会议论文 9 专利 18 著作 1
钒钛资源冶金过程有价组元强化迁移规律及分离理论
期刊论文 12 专利 6
同项目期刊论文
从红土镍矿镍铁渣中分离浸取镍铬工艺
褐铁型红土矿碱浸渣的常压酸浸工艺条件优化
蛇纹石型红土矿常压酸浸实验研究
Activation pretreatment of limonitic laterite ores by alkali-roasting using NaOH
Equilibrium Solubility Modeling of CO2 in Na2Cr2O7 Solutions
Preparation of Cr2O3 precursors by hydrothermal reduction in the abundant Na2CO3 and Na2CrO4 solutio
Synthesis of submicron spherical Fe MCM-48 with actual gyroid like structure
Activation pretreatment of low-grade Ti-slag by alkali roasting: Anticaking technique and kinetics o
Extraction of iron (III) from chloride leaching liquor with high acidity using tri-n-butyl phosphate
An extraction process to recover vanadium from low-grade vanadium-bearing titanomagnetite
Formation of Cr(VI) compounds during the thermal decomposition of amorphous chromium hydroxide
Pd nanoparticles supported on PDDA-functionalized Ti4O 7 as an effective catalyst for formic acid el
Removal of silicon in acid leaching and flocculation processes during zirconium oxychloride octahydr
Pt catalyst supported on titanium suboxide for formic acid electrooxidation reaction
Influence of Na2CO3 as additive on the direct reduction of boron-bearing magnetite concentrate
Recovery of titanium from undissolved residue (tionite) in the titanium oxide industry via NaOH hydr
连续分解锆英砂烧结料水洗工艺研究
Analysis of water leaching and transition processes in zirconium oxychloride octahydrate production
Electrocatalysis of carbon black- or poly(diallyldimethylammonium chloride)-functionalized activated
高砷烟道灰预处理水浸液中锌砷分离
LaXCoO_3(X=Mg,Ca,Sr,Ce)催化剂的制备及其催化乙醇水蒸气重整制氢
Preparation of activated carbon hollow fibers from ramie at low temperature for electric double-laye
Desilication from titanium-vanadium slag by alkaline leaching
铬酸钠碱性液中拜耳石的结晶行为(英文)
铬盐生产工艺中除铝方法的研究进展
Extraction of Al and K salts from associated alunite tailings by an acid calcination-water leaching
Aqueous Carbonation of Steel Slag: A Kinetics Study
采用阴离子膜电解法从红土镍矿常压浸出液中制备金属镍
铬盐生产工艺中除铝方法研究进展
Recovery of Ni, Co, Mn, and Mg from nickel laterite ores using alkaline oxidation and hydrochloric a
Mineralizer effects on the synthesis of amorphous chromium hydroxide and chromium oxide green pigmen
Dechromization and dealumination kinetics in process of Na2CO3-roasting pretreatment of laterite ore
Design and simulation of a green chromate compound production process
草酸浸出Na8Ti5O14制备草酸氧钛钠的工艺
Preparation and mechanism of TiO2-coated illite composite pigments
Structural control of Na2TiO3 in pre-treating natural rutile ore by alkali roasting for TiO2 product
Preparation of alumina from NaOH-NaAlO2-Na2CrO4-H2O solutions by carbonization process
Study on Lithium Insertion in Lepidocrocite and lambda-MnO2 Type TiO2: A First-Principles Prediction
Decomposition Kinetics of Titania Slag in Eutectic NaOH-NaNO3 System
Controlling the formation of Na2ZrSiO5 in alkali fusion process for zirconium oxychloride production
Application of mathematical models for ion-exchange removal of calcium ions from potassium chromate
A two-step zircon decomposition method to produce zirconium oxychloride: alkali fusion and water lea
临沂低品味钛矿的矿物组成及铁钛元素的分布状态
Mechanism and kinetics of titanium hydrolysis in concentrated titanyl sulfate solution based on infr
Characterization and atmospheric hydrochloric acid leaching of a limonitic laterite from Indonesia
Preparation of nanosized anatase TiO2-coated illite composite pigments by Ti(SO4)2 hydrolysis
Effect of ZnCl2 impregnation concentration on themicrostructure and electrical performance of ramie-
Removal of zirconium from hydrous titanium dioxide
磷酸活化焙烧-酸浸法富集低品位还原钛渣
氢氧化钠熔盐分解钛渣制备二氧化钛的热力学分析
碳化法制备重铬酸钠工艺优化
铬酸钠碳化生产重铬酸钠工艺的热力学模拟研究
CO2在Na2Cr2O7溶液中的平衡溶解度模型
分段进气多级环流反应器流动与传质特性研究
钒钛磁铁精矿直接还原过程中金属铁颗粒长大特性
临沂低品位钛矿的矿物组成及铁钛元素的分布状态
Leaching of vanadium, sodium, and silicon from molten V？Ti-bearing slag obtained from low-grade vanadium-bearing titanomagnetite
A novel process for the recovery of iron,titanium,and vanadium from vanadium-bearing titanomagnetite:sodium modification–direct reduction coupled process
亚熔盐法铬酸盐模拟浸出液中三水铝石的结晶行为
铬酸钾电解-结晶制备重铬酸钾的工艺
碱度对高铬型钒钛矿烧结过程的影响
Removal of zirconium from hydrous titanium dioxide
磷酸活化焙烧-酸浸法富集低品位还原钛渣
高温微波冶金反应器的研究现状及发展趋势
钒钛磁铁精矿的预氧化研究
直接还原含钛炉渣亚熔盐法制备钛白粉工艺研究
临沂低品位钛矿的矿物组成及铁钛元素的分布状态
含钛高炉渣叶面肥的大豆栽培实验研究
碳酸钠碱熔处理褐铁型红土镍矿的热力学分析与实验研究
从红土镍矿镍铁渣中分离浸取镍铬工艺
Innovative technology for processing saprolitic laterite ores by hydrochloric acid atmospheric press
Formation of Cr(VI) compounds during the thermal decomposition of amorphous chromium hydroxide.
铬盐生产工艺中除铝方法的研究进展
Activation pretreatment of limonitic laterite ores by alkali-roasting method using sodium carbonate
Research development of aluminum removal in chromium compound production
Crystallization of gibbsite from synthetic chromate leaching solution in sub-molten salt process
采用阴离子膜电解法从红土镍矿常压浸出液中制备金属镍
Precipitation of alpha-Fe2O3 and recovery of Ni and Co from synthetic laterite-leaching solutions
Leaching metals from saprolitic laterite ore using a ferric chloride solution
Crystallization behaviors of bayerite from sodium chromate alkali solutions.
Dechromization and dealumination kinetics in the process of Na2CO3-roasting pretreatment of laterite
Extraction of metals from saprolitic laterite ore through pressure hydrochloric-acid selective leach
亚熔盐法铬酸盐模拟浸出液中三水铝石的结晶行为
期刊信息
  • 《过程工程学报》
  • 北大核心期刊（2011版）
  • 主管单位:中国科学院
  • 主办单位:中国科学院过程工程研究所
  • 主编：张锁江
  • 地址：北京市海淀区中关村北二街1号过程大厦
  • 邮编：100190
  • 邮箱：CJPE@HOME.IPE.AC.CN GCGC@HOME.IPE.AC.CN
  • 电话：010-62554658
  • 国际标准刊号：ISSN：1009-606X
  • 国内统一刊号：ISSN：11-4541/TQ
  • 邮发代号:80-297
  • 获奖情况:
  • 国家中文核心期刊,中国科学院核心期刊,中国期刊方阵“双效”期刊,中国科学院优秀期刊
  • 国内外数据库收录:
  • 俄罗斯文摘杂志,美国化学文摘（网络版）,荷兰文摘与引文数据库,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊（2004版）,中国北大核心期刊（2008版）,中国北大核心期刊（2011版）,中国北大核心期刊（2014版）
  • 被引量:11515