本文以SiC粉末、烧高岭土、AI(OH)2粉末为主要原料,采用添加造孔剂法制备了多孔碳化硅/莫来石复合陶瓷,研究了造孔剂、烧结助剂、温度对多孔碳化硅/莫来石复合陶瓷性能的影响,并分别用XED和SEM分析晶相组成和断面显微结构。结果表明:随着石墨含量的增加,气孔率呈递增趋势,而抗弯强度的变化则相反。当Y2O3含量为1.5%,石墨含量为15%时,在1350℃下保温5h制备的样品抗折强度为34.31MPa,,其孔隙率达到46.15%。
In this experiment, porous silicon cabide/mullite composite ceramics were prepared by adding pore-forming material method from SiC powder, calcined kaolin and aluminum hydroxide powder. The influence of pore-forming material, sintering additives, and sintering temperatures on the properties of porous silicon cabide/mullite composite ceramics were investigated. The grain phases and the fracture surface micrograph were analyzed with XRD and SEM, respectively. The results show that:porosity showed an increasing trend, while the opposite change in flexural strength with the increase of the graphite content. The sample sintered at 1350 ℃ for 3 h with 1.5% Y203 and 15% graphite exhibits properties: flexural strength of 34.31 MPa was achieved at a porosity of 46.15%.