采用提拉法成功制备出高纯铜(Ca)单晶,最大尺寸为4,15mm×60mm。采用化学机械抛光(CMP)方法对Cu单晶基片进行抛光,借助光学显微镜、表面轮廓仪和扫描探针显微镜分析了基片表面形貌、表面粗糙度与表面均匀性,并探讨了抛光压力、表面活性剂和抛光垫对基片表面抛光的影响,结果表明:采用CMP加工后的铜单晶基片表面无宏观划痕、加工均匀性好,基片表面粗糙度醌为0.921nm。
The bulk Cu single crystal with the size of Ф15 mm × 60 mm was prepared by Czochralski technique. Cu single crystal wafers were polished by a so-called chemical-mechanical polishing (CMP) method. The surface morphology, uniformity and roughness of as-polished wafer were analyzed by optical microscopes, surface profiler and scanning probe microscopy. The influence of polishing pressure, surface active agent and polishing pad on polishing quality was discussed. The results indicate that there is no macroscopic scratch on the as-polished wafer surface with good uniformity and the Ra value of Cu wafer is 0.921 nm in the final finishing polishing process.