利用透射电镜对掺氮(NCZ)和普通(CZ)直拉硅单晶中的原生氧沉淀进行研究.研究表明,在NCZ样品中,有高密度的粒径为5nm的氧沉淀生成,而在CZ样品中,没有观察到这种氧沉淀.初步认为,这种细小的氧沉淀是以650℃低温下形成的N-0复合体为核心在随后的冷却过程中形成.
The grown-in oxygen precipitates in conventional Czochralski (CZ) silicon and nitrogen-doped Czochralski (NCZ) silicon have been investigated by means of transmission electron microscopy (TEM). Tiny oxygen precipitates about 5 nm in size were observed in the NCZ specimens. It is believed that the oxygen precipitates may have grown from the heterogeneous nuclei of nitrogen-related complexes formed at a low temperature of 650℃.