以三氟苯乙酮、溴代烃和异氰酸酯为原料,在金属锌的促进下,室温条件下通过三组分“一锅法”反应合成了新型的含三氟甲基氨基甲酸酯类化合物。产品结构经过IR、H1 NMR、C13 NMR和HRMS进行了确认。
In the promotion of metallic zinc, a novel carbamate containing trifluoromethy was synthesised by 2,2,2-Trifluoroacetophenone , brominated hydrocarbons and isocyanate in “one pot” at room temperature .The structure of the new carbamate were confirmed by IR , 1H NMR, 13 C NMR, HRMS.