采用放电等离子技术(SPS)烧结制备出纳米复合Ti(C,N)基金属陶瓷材料。用光学显微镜、扫描电镜和能谱仪等对烧结体的孔隙率、微观组织和断口形貌等进行了观察,并对不同条件下材料的力学性能进行了对比分析。结果表明:直接升温到1250℃保温8min可获得较好的力学性能;在显微结构中,除了黑芯/白环的结构外,还存在着白芯/黑环结构;孔洞和大颗粒硬质相为主要的断裂源,断裂方式以沿晶断裂为主,同时存在着解理断裂和穿晶断裂。
OM, SEM, EDX and other techniques were used to analyze the porosity, microstructure and fractography of nano-composite Ti(C, N)-hased cermets produced by spark plasma sintering(SPS). The mechanical properties of Ti(C, N)-hased cermets produced in different conditions were discussed. At 1 250℃ for 8min by elevating directly, fairly good mechanical performance could be obtained. Except the microstructure of black core/ white rim, white core/black rim was also presented, which resulted from the existence of nano-powders which changed the evolution of microstructure. The fracture mainly originated from cavities and the intergranular fracture was the leading fracture mode, besides the cleavage fracture and transgranular fracture.