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羊肉纯度电子舌快速检测方法
  • ISSN号:1002-6819
  • 期刊名称:农业工程学报
  • 时间:2013.10.10
  • 页码:255-262
  • 分类:TS251[轻工技术与工程—农产品加工及贮藏工程;轻工技术与工程—食品科学与工程]
  • 作者机构:[1]浙江大学生物系统工程与食品科学学院,杭州310058, [2]西北民族大学生命科学与工程学院,兰州730024
  • 相关基金:国家科学部支撑计划(2012BAD29B02-4); 国家自然科学基金(31071548); 博士点基金20100101110133
  • 相关项目:肉品品质的电子鼻检测机理研究
中文摘要:

为实现掺假羊肉的快速、客观评价,利用电子舌对混入不同比例鸡肉的掺假羊肉糜进行检测及定性和定量分析。3种浸提溶液分别浸提,样品量均对电子舌传感器的响应影响极显著;以数据点重复性和聚类效果为依据,采用主成分分析方法确定了电子舌检测羊肉糜样品的较佳条件为0.1 mol/L KCl溶液浸提15 g肉糜样品。在此较佳条件下,对混入不同比例鸡肉的掺假羊肉进行检测,结果表明:采用主成分分析和典则判别分析,前2个主成分累积贡献率均超过80%,电子舌均能很好地区分混入不同比例鸡肉的羊肉糜样品;采用多元线性回归分析和偏最小二乘回归分析建立的定量预测模型能有效预测混入的鸡肉比例(R2〉0.99,RMSE〈3%)。试验表明:电子舌在羊肉掺入鸡肉的鉴别中具有可行性,研究结果可为羊肉掺假鉴别提供参考。

英文摘要:

Cheaper animal protein, such as Chicken as an example, has been fraudulently used as a substitute for more expensive animal proteins, like mutton and beef. The adulteration of mutton has attracted increasing attention. It requires reliable methods for the authentication of mutton adulteration. An electronic tongue with chemically modified field-effect-transistor sensors was employed to analysis the adulteration of chicken in minced mutton. The effects of sample weight on the sensor responses of electronic tongue were studied at three different extraction solutions. Analysis of variance found that the sample weight affected the responses of the sensor significantly. With the help of Principle component analysis (PCA), the optimum experimental parameters were acquired: 15 g sample extracted by 100 mL KC1 solution. The adulterated mutton was made by mixing mutton with chicken at levels of 0, 20%, 40%, 60%, 80%, and 100% by weight, respectively. With the optimum experimental parameters, 168 samples of adulterated mutton were detected, and the signals were analyzed by pattern recognition techniques to build models for classification of adulterated mutton with different content of chicken, and prediction of the content of chicken in minced mutton With PCA, the adulterated mutton samples were grouped according to their content of chicken with good classification results, except that samples containing 80% and 100% chicken partially overlapped with each other. Better classification results were found when canonical discriminant analysis (CDA) was employed, as samples containing 80% and 100% chicken were clearly grouped and separated. Multiple linear regression (MLR) and Partial least square analysis (PLS) were employed to build the predictive model for the content of chicken adulterated into minced mutton. Both models could predict the adulteration with a high determination coefficient as high as 0.9925 and 0.9923, respectively. MLR was more effective for the prediction of chicken content. The E-nose p

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期刊信息
  • 《农业工程学报》
  • 北大核心期刊(2011版)
  • 主管单位:中国科学技术协会
  • 主办单位:中国农业工程学会
  • 主编:朱明
  • 地址:北京朝阳区麦子店街41号
  • 邮编:100125
  • 邮箱:tcsae@tcsae.org
  • 电话:010-59197076 59197077 59197078
  • 国际标准刊号:ISSN:1002-6819
  • 国内统一刊号:ISSN:11-2047/S
  • 邮发代号:18-57
  • 获奖情况:
  • 百种中国杰出学术期刊,中国精品科技期刊,中国科协精品科技期刊工程项目期刊,RCCSE中国权威学术期刊
  • 国内外数据库收录:
  • 俄罗斯文摘杂志,美国化学文摘(网络版),英国农业与生物科学研究中心文摘,荷兰文摘与引文数据库,美国工程索引,美国剑桥科学文摘,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),英国食品科技文摘,中国北大核心期刊(2000版)
  • 被引量:93231