以铝粉、AlCl3·6H2O和水为原料,通过调整原料配比、水热反应和陈化的温度和时间,经蒸发、结晶、晶化,制成一种组成为Al17O16(OH)16Cl3的氯化十七聚铝(Al17),采用XRD和化学分析,对其进行了初步表徵。
A novel heptadeca-meric polyaluninum chloride, Al17O16(OH)16Cl3 , was prepared in a hydro-thermal condition of 128℃ by using aluminum powder, AlCl3-6H2O and water as reactants, adjusting the recipe, reacting and aging temperature and time, and evaporating, crystallizing and crystallization. The result product was characterized by XRD and chemical analysis.