诺卜醇经Ni(R)催化氢化合成氢化诺卜醇,氢化诺卜醇与7种羧酸进行酯化反应合成7种羧酸酯,产率均在90%以上,GC纯度达98%.对合成的羧酸酯均进行了IR、1H NMR、13C NMR与MS分析。
Hydronopol was prepared from the hydrogenation of nopol in the presence of Raney Ni. And hy- dronopol reacts with 7 different kinds of carboxylic acids to produce new compounds of hydronopyl carboxylic ether series. The yield of the products (GC content were over 98%) were not less than 90%. Identification and structural analysis were done using IR, 1H NMR, 13C NMR and MS methods.