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中文摘要：
本项目以毛细管电泳-质谱（CE-MS）和加压毛细管电色谱－质谱（PCEC－MS）联用新技术为基础，对天然药物复杂样品体系的分离与检测进行了一系列新技术、新方法的研究。项目以一系列创新性基础研究为技术支撑，包括PCEC－MS联用新技术；ESI垂直型鞘液接口喷雾设计和零电位连接设计；PCEC独具特色的在线、灵敏、快速预浓缩进样和在线富集；CEC柱的动态涂层和整体柱填充等技术，实现对复杂体系中痕量目标物的定性定量分析，以及对天然药物太子参中代表性化合物指标成分的定量，建立科学的太子参的化学特征识别图谱和药材分类图谱，以及定性评价和成分定量分析的方法。
结论摘要：
英文主题词capillary electrochromatography; mass spectrometry; natural medicines; pseudostellariae;
成果综合统计
期刊论文
会议论文
专利
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著作
期刊论文
Determination of thyreostatics in animal feeds by capillary electrophoresis with electrochemical det
Preparation and Evaluation of the Highly Cross-linked Poly(1-hexadecene-co-TMPTMA) Monolithic Column
Simultaneous analysis of endogenetic and ectogenic plant hormones by pressurized capillary electroch
A new mixed micellar electrokinetic chromatography method for analysis of natural and synthetic anab
A simple capillary electrophoresis with electrochemical detection method for determination of the hy
Rapid analysis of peptides and amino acids by CE-ESI-MS using chemically modied fused-silica capilla
Rapid separation and sensitive detection method for β-blockers by pressure-assisted capillary electr
Design and fabrication of a micro-electrochemiluminescent cell for the study of ionic liquid-mediate
Electrochemiluminescent behavior of T ris(2,2-bipyridine) ruthenium(II) / triethylamine in Ionic Liq
Pressure-assisted capillaryelectrochromatography with electrospray ionization-mass spectrometry base
会议论文
Determination of organophosphorus pesticide residues in tea by solid-phase extraction with gas chrom
HF-LPME with in-situ derivatization agonists and blockers in urine following determination by gas ch
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