极其细小的铬的氧化物粉末被新奇煤气固体的减小反应准备。Na2CrO4 第一在 400600 擬 与氢被减少吗??
The ultra-fine chromic oxide powder was prepared by a novel gas-solid reduction reaction.Na2CrO4 was firstly reduced with hydrogen at 400-600 ℃.The obtained reduction products,mainly the mixture of NaCrO2 and sodium hydroxide(NaOH),were converted into chromic oxide through hydrolysis followed by calcination.The obtained chromic oxide product was characterized by powder X-ray diffraction(XRD) and SEM.The results show that the hydrolysis process of sodium chromite is the key step and lower reduction temperature helps intensify the hydrolysis process.