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新型泡沫碳化硅塔板的流体力学及传质性能
  • ISSN号:0493-2137
  • 期刊名称:天津大学学报(自然科学与工程技术版)
  • 时间:2014
  • 页码:155-162
  • 分类:TQ053.5[化学工程]
  • 作者机构:[1] 天津大学化工学院,天津 300072, 天津大学精馏技术国家工程研究中心,天津 300072, [2] 天津大学化工学院,天津,300072, [3] 中国科学研究院金属所,沈阳,110016
  • 相关基金:国家自然科学基金资助项目(21336007,21176172);国家科技支撑计划资助项目(2011BAE03807);长江学者和创新团队发展计划资助项目(IRT0936).
  • 相关项目:新型多孔碳化硅泡沫传质体塔盘的性能研究与结构优化
中文摘要:

利用碳化硅泡沫材料的孔隙率高、表面积大、强度大、耐腐蚀和不漏液等优点,将其应用到塔板上,开发出新型整体多孔碳化硅泡沫塔板。将一定孔径的碳化硅泡沫材料制作成厚度为12,mm 的块状塔板,在φ600,mm 的塔内进行流体力学实验,测定了干板和湿板压降、雾沫夹带及漏液量等参数;以环己烷-正庚烷为标准物系在φ300,mm的传质塔中进行了传质实验研究,在常压、全回流条件下测定了全塔效率来表征塔板传质效率;选择按工业设计标准制成的筛板与其性能进行比较。结果表明:泡沫孔径为2,mm 的塔板压降过高;泡沫孔径为4,mm 的塔板漏液较多,且出现不均匀漏液;而孔径为3,mm及3~4,mm组合的两种新型塔板具有压降低、雾沫夹带少、漏液少和全塔效率高等特点,是流体力学及传质性能优良的新型泡沫塔盘。

英文摘要:

With its advantages of high porosity,high surface area,high mechanical strength,good resistance to corrosion and no-leakage construction,SiC foams have been applied to tray columns to develop a series of novel trays. SiC foams with the thickness of 12,mm and various sizes of pores were used for making trays in the hydrody-namic experiments. Performance parameters including pressure drop for the dry and wet trays,entrainment and the quantity of leaking liquid were measured in a 600,mm external diameter column. The mass transfer efficiency in terms of the overall column efficiency was determined by total reflux experiments using a mixture of n-heptane and cyclo-hexane at atmospheric pressure in a column of 300,mm external diameter. Sieve trays designed according to the indus-trial standards were chosen for the performance comparison with the SiC foam trays. Results show that the pressure drop of the tray with 2,mm pore diameter is too high;there is a serious leaking of liquid for the tray of 4,mm pore diameter with the phenomenon of mal-distributed weeping;compared with sieve tray,the trays with the sizes of pores being 3,mm and 3-4,mm combination performed better with low pressure drop,small entrainment,little leaking of liquid and high overall column efficiency.

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期刊信息
  • 《天津大学学报:自然科学与工程技术版》
  • 北大核心期刊(2011版)
  • 主管单位:
  • 主办单位:天津大学
  • 主编:单平
  • 地址:天津市南开区
  • 邮编:300072
  • 邮箱:
  • 电话:022-27403448
  • 国际标准刊号:ISSN:0493-2137
  • 国内统一刊号:ISSN:12-1127/N
  • 邮发代号:6-27
  • 获奖情况:
  • 中国期刊方阵双效期刊
  • 国内外数据库收录:
  • 美国数学评论(网络版),美国剑桥科学文摘,中国中国科技核心期刊,中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版)
  • 被引量:6410