欢迎您！东篱公司
退出
-
申报数据库
-
立项数据库
-
成果数据库
-
项目获奖数据库
中文摘要：
通过设计反相微乳液反应体系，在水热条件下缓慢氧化SnF2，合成了单分散的四方形SnO2纳米晶．利用X射线多晶粉末衍射、扫描电镜、高分辩透射电镜对合成样品的形貌和结构进行了表征．实验结果表明，通过控制油胺的添加量调控微乳液水相的pH值，可以对SnO2的形貌进行调控．使用适当量的油胺，可以获得分散性极好、大小为10nm左右的规则四方SnO2纳米晶．合适的pH值有利于晶核的定向生长，从而在微乳液反应器中形成了规则的SnO2四方纳米晶．
英文摘要：
A nanosized reverse microemulsion reactor was designed for the fabrication of monodispersed SnO2 nanosquares by oxidation of SnF2 under hydrothermal conditions. As-prepared samples were characterized by X-ray diffraction, scanning electron microscope, transmission electron microscope and high resolution transmission elec- tron microscope. The results show that the morphology of the SnO2 nanocrystals can be controlled by regulating the amount of the used oleylamine which direct influenced the pH values of the aqueous phase. Well monodispersed SnO2 nanosquares with the size around 10 nm can be obtained. A proper pH value could benefit the oriented attachments of the crystalline seeds which gradually grew into a square-plate NCs shape in the microemulsion reactor.
同期刊论文项目
同项目期刊论文
~Phase transformation synthesis of novel Ag2O/Ag2CO3 heterostructures with high visible light effici
~Hydrothermal synthesis and characterization of novel PbWO4microspheres with hierarchical nanostruct
A sonochemical route to fabricate the novel porous F, Ce-codoped TiO2 photocatalyst with efficient p
Thermal stability, microstructure and photocatalytic activity of the bismuth oxybromide photocatalys
~Stable Au25(SR)18/ TiO2 Composite Nanostructure with Enhanced Visible Light Photocatalytic Activity
~Novel hollow Pt-ZnO nanocomposite microspheres with hierarchical structure and enhanced photocataly
~Novel noble metal (Rh, Pd, Pt)/BiOX(Cl, Br, I) composite photocatalysts with enhanced photocatalyti
~Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under vis
~Preparation of Co/CexTi1-xO2 Catalysts and Their Catalytic Performance in the Catalytic Partial Oxi
Fast fabricate Co3O4 or CuO/BiVO4 composite photocatalysts with high crystallinity and enhanced phot
An efficient palladium membrane reactor for increase the yield of styrene in ethylbenzene dehydrogen
Preparation of bismuth oxyiodides and oxides and their photooxidation characteristic under visible/U
期刊信息
位置：