用磁控溅射技术制备不同调幅波长(L)的W(Mo)/Cu纳米多层膜,所制膜系在60keV氦离子(He^+)辐照条件下注入不同剂量:0,1×10^17He^+/cm^2,5×1017He^+/cm^2.用X射线衍射仪(XRD)和高分辨透射电子显微镜(TEM)表征W(Mo)/Cu纳米多层膜辐照前后微观结构.研究结果表明:1)He^+离子轰击引起温升效应是导致沉积态亚稳相β-W转变成稳态α-W相的主因,而与调幅波长无明确关联;2)纳米多层结构中W(Mo)和Cu膜显现出的辐照耐受性与调幅波长相关,调幅波长越小,抗He^+的辐照性能越强;3)在5×10^17He^+/cm^2注入条件下,观察到He团簇/泡在纳米结构W(Mo)和Cu膜中的积聚行为存在明显差异:在W(Mo)膜中He团簇/泡的分布与晶粒取向相关,He团簇/泡倾向于沿W(211)晶面分布;而Cu膜非晶化且He团簇/泡在其体内呈均匀分布.
W(Mo, 9.8 at.%)/Cu nanometer multilayer films of different individual layer thickness were prepared by RF magnetron sputtering, which were irradiated by 60 keV He + ions at ion fluence from 0 to 5 × 10^17 He^+/cm^2. Microstructures of nanometer multilayer W(Mo)/Cu films were investigated by high-resolution transmission electron microscope (HRTEM) and X-ray diffraction (XRD) before and after irradiation. Experimental results indicate that: (1) The phase transformation of β-W (A-15) into steady state α-W can be attributed to the bombardment effect of energetic He ions on the surface of films, leading to phase-transition temperature during irradiation. (2) The irradiation tolerance of W(Mo)/Cu multilayer film was found to depend on the individual layer thickness. (3) At the fluence of 5 × 10^17 He^+/cm^2, the HRTEM results reveal that the behavior of helium cluster/bubble in the W(Mo) film is obviously different from that in the Cu film. It is interesting that the distribution of helium cluster/bubble is related to the grain orientation of W(Mo) film and tends to distribute along W (211) plane. However, Cu film is completely amorphized and helium cluster/bubble is evenly distributed in it.