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高分辨X射线衍射表征氮化镓外延层缺陷密度
  • ISSN号:1000-324X
  • 期刊名称:《无机材料学报》
  • 时间:0
  • 分类:O657[理学—分析化学;理学—化学]
  • 作者机构:[1]山东大学晶体材料国家重点实验室,济南250100
  • 相关基金:国家高技术研究发展计划863项目(2014AA032601); 国家自然科学基金(51323002,61327808,51321091)
中文摘要:

利用高分辨X射线衍射方法,分析了在4H-Si C(0001)面上采用金属有机物化学气相沉积(MOCVD)生长的Ga N薄膜的位错。采用对称面衍射和斜对称面衍射等方法研究了晶面倾转角、面内扭转角、晶粒尺寸和晶面弯曲半径等参数,通过排除仪器、晶粒尺寸及晶面弯曲对摇摆曲线半高宽的影响,从而获得Ga N薄膜的螺位错密度和刃位错密度分别为4.62×10^7 cm^-2和5.20×10^9 cm^-2,总位错密度为5.25×10^9 cm^-2。

英文摘要:

The measurement of dislocation densities in heteroepitaxial semiconductor Ga N film is important for the developement of blue light-emitting diodes, laser diode and high temperature, high-frequency electronic devices. As there is no matching substrate material, Ga N thin films prepared by epitaxial growth often contain a large number of defects, most of which are edge dislocations. High resolution X-ray diffraction method and the mosaic model were used to measure and analyze the dislocation density of Ga N film fabricated by metal organic chemical vapor deposition(MOCVD) on a 4H-Si C substrate with an Al Ga N buffer layer. The crystal face tilting angle, in-plane twisting angle, grain size and crystal bending radius were investigated by symmetry and oblique symmetry diffraction methods. By eliminating the instrumental broadening width(mainly the incident beam divergence), grain size and wafer curvature influenced on the contribution to the full width at half maximum of rocking curves, Screw dislocation density and edge dislocation density of the Ga N film were accurately determined to be 4.62×10^7 cm^-2 and 5.20×10^9 cm^-2, respectively. The total dislocation density was 5.25×10^9 cm^-2. There were less than 1% screw dislocations, and the ratio of mixed to edge dislocation failed to be determined.

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期刊信息
  • 《无机材料学报》
  • 北大核心期刊(2011版)
  • 主管单位:中国科学院
  • 主办单位:中国科学院上海硅酸盐所
  • 主编:郭景坤
  • 地址:上海市定西路1295号
  • 邮编:200050
  • 邮箱:wjclxb@mail.sic.ac.cn
  • 电话:021-52411302
  • 国际标准刊号:ISSN:1000-324X
  • 国内统一刊号:ISSN:31-1363/TQ
  • 邮发代号:4-504
  • 获奖情况:
  • 获"中国百种杰出学术期刊"称号
  • 国内外数据库收录:
  • 美国化学文摘(网络版),荷兰文摘与引文数据库,美国工程索引,美国剑桥科学文摘,美国科学引文索引(扩展库),日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),瑞典开放获取期刊指南,中国北大核心期刊(2000版)
  • 被引量:21274