采用对喷静电纺丝法制备了PVP/TiO2/TPEE/Zn(CH3COO)2纳米纤维,分别在500℃、550℃、600℃、650℃和700℃锻炼5h,得到不同煅烧温度下的TiO2/ZnTiO3复合纳米纤维光催化剂,利用热重-差热分析法(TG-DTA)、扫描电子显微镜(SEM)、X射线衍射仪(XRD)对样品进行了表征,并研究了该催化剂在300W的紫外灯下催化亚甲基蓝(MB)降解的活性。结果表明,当煅烧温度为550℃时,TiO2/ZnTiO3复合纳米纤维催化剂的光催化活性最高。
PVP/TiO2/TPEE/Zn(CHaCOO)2 nanofibers were prepared by two-spinneret electrospinning. The as-spun fibers were calcined at 500℃, 550℃, 600℃, 650℃, and 700℃ for 5h, and TiO2/ZnTiO3 composite nanofibers were obtained. The fabricated samples were characterized by thermogravimetry-differential thermal analysis (TG- DTA), X-ray diffraction (XRD), and scanning electron microscopy (SEM). The processes of the photocatalytic deg- radation of methylene blue (MB) at ultraviolet lamp by the prepared nanofibers photocatalyst were investigated. The results show that TiO2/ZnTiO3 composite nanofibers calcined at 550℃ have the highest photocatalytie property.