目的:研究梅花挥发油化学成分.方法:采用水蒸气蒸馏法提取梅花挥发油,气相色谱-质谱法对挥发油成分进行分离和鉴定,面积归一化法测定各成分的相对百分含量.结果:从梅花挥发油中共分离得到71个色谱峰,经NIST2008质谱数据库检索鉴定了其中51个成分的结构.结论:梅花挥发油化学成分包括醛类、酯类、有机酸、醇类和脂肪类化合物,其中主要成分按相对含量由高到低排序依次为苯甲醛(42.93%),苯甲酸苄酯(9.16%),二十一烷(7.96%),二十三烷(7.39%),棕榈酸(3.62%)和3-烯丙基-6-甲氧基苯酚(2.51%).
Objective:To study the chemical constituents of the volatile oil from the flower bud of Prunus mume.Method:The volatile oil was extracted by steam distillation and analyzed by GC-MS.The composition of the volatile oil was determined according to peak area normalization method.Result:Total 51 compounds were isolated and identified from the volatile oil of the flower bud of P.mume.Conclusion:Chemical constituents of the volatile oil from the flower bud of P.mume included aldehydes,esters,organic acids,alcohols and fatty compounds.The main components were benzaldehyde (42.93%),benzyl benzoate (9.16%),heneicosane (7.96%),tricosane (7.39%),n-hexadecanoic acid (3.62%) and 3-allyl-6-methoxyphenol (2.51%).