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中文摘要：
2,7-二叔丁基咔唑与氨基硫脲经缩合反应合成了一种新型咔唑希夫碱——4-[9-（3,6-二叔丁基）咔唑基]苯甲醛缩氨基硫脲（1）,其结构经1H NMR,IR,MS,XRD和元素分析表征.1属单斜晶系,P21/c空间群,晶胞参数a=6.386 1（17）（A）,b=38.587（10）（A）,c=12.741（3）（A）,β=119.759（10）.,V=2 725.6（12）（A）3,Dc =1.171 g·cm-3,Z=4,F（000） =1 024,μ=0.143 mm-1,R1 =0.060 5,wR2 =0.161 6.
英文摘要：
A novel carbazole Sehiff base, 1 - [ 4 - （ 3,6 -di-tert-butyl-gH-earbazol-9-yl） phenyl ] methyl- ene thiosemicarbaide（ 1）, was synthesized by condensation of 2,7-di-tert-gH-carbazol with thiosemi- carbazone. The structure was characterized by I H NMR, IR, MS, XRD and elemental analysis. 1 belongs to monoclinic system, space group P21/c with a=6.386 1（17）（A）,b=38.587（10）（A）,c=12.741（3）（A）,β=119.759（10）.,V=2 725.6（12）（A）3,Dc =1.171 g·cm-3,Z=4,F（000） =1 024,μ=0.143 mm-1,R1 =0.060 5,wR2 =0.161 6.
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