采用聚乙二醇(PEG(2000))辅助的水热合成法制备出了粒径较为均匀的花状氧化锌纳米团簇,并用SEM、XRD对其进行了表征。实验结果表明,表面活性剂(PEG-2000)和氨水的加入量对ZnO纳米团簇的形貌有直接的影响;将ZnO纳米团簇均匀涂在导电玻璃的导电面上,在一定温度下煅烧后制成纳米团簇膜电极,并进行了光电化学研究。
In this paper , flower-like ZnO nanocomplex which have uniform partical size was prepared with PEG- assisted hydrothermal method, and the products were characterized with SEM,XRD. The results showed that addition of surfactant(PEG 2000) and liquid ammonia had a direct influence on pattern of ZnO nanocomplex; the ZnO nanocomplex/ITO film were sintered at different temperatures. And photoelectrochemical properties of the ZnO nanocomplex were studied.