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不同加工方法对泸州山银花品质影响的研究
  • ISSN号:0254-1793
  • 期刊名称:《药物分析杂志》
  • 时间:0
  • 分类:R917[医药卫生—药物分析学;医药卫生—药学]
  • 作者机构:[1]泸州医学院药物与功能性食品中心, [2]泸州医学院公共卫生学院,泸州646000
  • 相关基金:泸州市重点科技项目(泸市财企【2010】41号);泸州医学院2011年青年基金(2012026)
中文摘要:

目的:探讨不同加工方法对泸州山银花品质的影响,为泸州山银花加工方法的筛选提供依据。方法:采用阴干、晒干、真空干燥、远红外干燥、微波干燥、烘干6种方法加工山银花,对外观性状进行描述,采用高效液相色谱法测定山银花中新绿原酸、绿原酸、异绿原酸A、异绿原酸c的含量。色谱柱为KromasilC,。柱(250mm×4.6mm,5μm);流动相为乙腈-0.1%磷酸水溶液,梯度洗脱;检测波长326nm;柱温30℃;流速1mL·min^-1;进样量10μL。结果:6种加工方法中,真空干燥样品中新绿原酸、绿原酸、异绿原酸A及异绿原酸C的含量分别为0.094%、2.982%、1.804%、0.255%,高于其他5种方法所得样品;外观颜色和油润度均比其他5种方法好。结论:真空干燥方法得到的样品外观品相好,测得的新绿原酸、绿原酸、异绿原酸A及异绿原酸C含量高,明显优于其他干燥方法。

英文摘要:

To discuss the effects of different drying methods on officinal qualities of Flos Lonicerae. Methods :The following six methods were used:drying in the shade, drying in the sun, vacuum drying, far infrared drying, microwave drying, and oven drying. External qualities were studied and the contents of neochlorogenic acid, chlorogenic acid, on a Kromasile C sochlorogenic acid A and isochlorogenic acid s column(250 mm ×4.6 mm,5 μm)at 30℃. C were determined by HPLC. HPLC was performed The composition of mobile phase was acetonitrile - 0. 1% phosphoric acid with gradient elution,the flow rate was 1 mL · min-1 ,and the injection volume was 10 μL. Results:The content of neochlorogenic acid, chlorogenic acid, isochlorogenic acid A and isochl9rogenic acid C in the vacuum drying sample was 0. 094% ,2. 982% , 1. 804% and 0. 255% respectively, which was obviously higher than samples dried by other five methods;the color and texture of the vacuum drying sample was also better. Conclusion: The appearance and contents of chlorogenic acids of the vacuum drying sample are better than those of the others, indicating that the vacuum drying method is obviously better than the others.

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期刊信息
  • 《药物分析杂志》
  • 中国科技核心期刊
  • 主管单位:中国科协
  • 主办单位:中国药学会
  • 主编:金少鸿
  • 地址:北京天坛西里2号
  • 邮编:100050
  • 邮箱:ywfx@nifdc.org.cn
  • 电话:010-67058427
  • 国际标准刊号:ISSN:0254-1793
  • 国内统一刊号:ISSN:11-2224/R
  • 邮发代号:2-237
  • 获奖情况:
  • 四通杯全优期刊奖,92、97年获科协优秀期刊三等奖,96年影响因子全年第一
  • 国内外数据库收录:
  • 美国国际药学文摘,美国化学文摘(网络版),日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),英国英国皇家化学学会文摘,中国北大核心期刊(2000版)
  • 被引量:32603