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中文摘要：
建立了污泥、底泥及土壤样品中7种合成麝香的分析方法。采用加速溶剂萃取（ASE）提取,经硅胶/中性氧化铝复合层析柱净化后,浓缩并定容洗脱液,用GC-SIM-MS进行检测。本方法对替代物标样荧蒽-d10的回收率为89.7%～110.9%。以六氯苯-c13为内标,7种合成麝香的线性范围为0.6～100.0μg/kg。底泥和土壤中麝香的检出限为0.25～0.33μg/kg（S/N=3）;污泥中的检出限为2.9～3.3μg/kg（S/N=3）。基质加标回收实验的平均回收率为83.6%～105.1%;RSD为3.2%～9.8%。本方法准确、快速,可用于实际样品的检测。
英文摘要：
A rapid, simple accelerated solvent extraction （ASE） method has been developed to determine seven synthetic musks in sewage sludge, sediment and soil by GC-MS. After extraction, samples were cleaned up by silica gel/ neutral Al2O3column. Then final eluate was concentrated before injection. Identification was carried out by GC-MS in the Selective Ion Monitor （SIM） mode. Using the method, the recovery of fluenthene-d10, surrogate standard, was from 89.7% to 110.9%. The detection limits of musks were from 2.9 to 3.3 μg/kg in sewage sludge and 0.25-0.33 μg/kg in sediment and soil（S/N=3）. Using hexachlorobenzene （HCB） 13C6 as the internal standard, good linear calibrations were obtained in the range of 0.6-100 μg/kg. The average recoveries were in the range of 83.6%-105.1% when the spiked concentration was 10 μg/kg. The RSD ranged from 3.2% to 9.8%. The method is accurate during the inspection of synthetic musks in real samples.
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