欢迎您！东篱公司
退出
-
申报数据库
-
立项数据库
-
成果数据库
-
项目获奖数据库
中文摘要：
本文用TLC法对姜黄消痤搽剂中芳姜黄酮进行定性鉴别,用HPLC法对芳姜黄酮进行含量测定,使用waters C18高效液相色谱柱（4.6 mm×250 mm,5μm）,流动相为甲醇-水（80：20）,流速1.0 mL/min,柱温25℃,检测波长242 nm。结果显示TLC色谱中芳姜黄酮斑点清晰,分离效果良好;HPLC法中芳姜黄酮在0.101-3.232μg线性关系良好（R^2=0.9995）,平均回收率是100.6%,RSD=2.74%（n=6）。表明该方法稳定、可靠,可用于姜黄消痤搽剂的质量控制。
英文摘要：
To determine the original quality of Jianghuang Xiaocuo liniment,Ar-Turmerone was identified by TLC and quantified by HPLC,the chromatography was performed on the waters C18 cloumn（4. 6 mm × 250 mm,5 μm） in gradient. The mixture of methyl and water was used as the mobile phase at a flow rate of 1. 0m L / min,the detection wavelength was 242 nm and the column temperature was set at 25℃. The results showed that,TLC spots were clear and well-separated without negative interference. For quantification,the calibration curve of Ar-Turmerone was linear within the range of 0. 101-3. 232 μg（R^2 = 0. 999 5）,the average recovery was 100. 6%,and RSD was 2. 74%（n = 6）,indicating that the established method was simple,accurate,and reliable,thus might be used for quality controlling of Jianghuang Xiaocuo liniment.
同期刊论文项目
同项目期刊论文
期刊信息
位置：