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土壤、沉积物和植物样品中多环芳烃(PAHs)不同提取与净化方法比较

ISSN号：1672-2043
期刊名称：农业环境科学学报
时间：2011.12.20
页码：2399-2407
分类：X830.2[环境科学与工程—环境工程]
作者机构：[1]贵州民族学院化学与环境科学学院,贵阳550025, [2]南开大学环境科学与工程学院,环境污染过程与基准教育部重点实验室,天津300071, [3]Department of Biology and Environmental Science, School of LifeSciences, University of Sussex, Falmer, Brighton BN1 9QJ UK, [4]农业部环境保护科研监测所污染防治研究室农业部／天津市产地环境与农产品安全重点开放实验室,天津300191
相关基金：国家自然科学基金重点项目（40930739,21037002）
相关项目：土壤污染微界面过程及其分子诊断与调控原理

关键词： PAHS, 提取方法, 净化方法, 土壤样品, 沉积物样品, 植物样品, PAHs, extraction method, purification method, soil sample, sediment sample, plant sample

中文摘要：

系统分析和比较了土壤、沉积物和植物样品中多环芳烃（PAHs）的提取与净化方法,阐述和对比了索氏提取法、超声波提取法、超临界流提取法、固相提取与固相微提取法、固液提取法、微波辅助提取法、快速溶剂提取法等提取方法以及定量浓缩净化法、硅胶柱层析净化法、费罗里土柱层析净化法、氧化铝净化法、固相萃取（SPE）净化法等净化方法。旨在通过比较目前的提取和净化方法,展望将来提取与净化方法发展的新方向。

英文摘要：

Various extraction and purification methods for polycyclic aromatic hydrocarbons（PAHs） in soil,sediment and plant samples were systematically analyzed.The extraction methods including Soxhlet extraction,ultrasonic assisted extraction,supercritical fluid extraction,solid phase extraction,solid phase microextraction,solid-liquid extraction,cloud point extraction,shaking extraction,microwave assisted extraction and accelerated solvent extraction were expounded and compared.At the same time the purification methods were also reviewed,such as quantitative concentrated purification,silica column purification,Florisil column purification,alumina gel column purification,gel permeation chromatography purification and solid phase extraction（SPE） purification.The extraction and purification methods for plant samples were similar with those for soil and sediment samples.The most widely applied extraction methods for plants were Soxhlet extraction,ultrasonic assisted extraction,supercritical fluid extraction,accelerated solvent extraction,solid phase extraction and plant solvent extraction.The most widely applied purification methods for plants were silica column purification,saponification assisted silica column purification,gel permeation chromatography purification,solid phase extraction（SPE） purification and hollow fiber liquid micro-extraction.According to the comparison of the current extraction and purification methods,future developments for both of the methods were suggested.New equipments should be explored to reduce the inaccuracy of experiments.